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Determination of sulfur compounds, halogenated compounds individually and/or their sum, and formaldehyde in hydrogen by gas chromatography (GC-MS-TD)

Determination of sulfur compounds, halogenated compounds individually and/or their sum, and formaldehyde in hydrogen by gas chromatography (GC-MS-TD)

Methodology No.:

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Methodological guidelines in the form of a standard operating procedure, detailing the work involved in applying the analytical method for determining sulfur compounds, halogenated compounds individually and/or their sum, and formaldehyde in hydrogen. The procedure was developed, implemented, and optimized based on research into analytical gas determinations in a hydrogen matrix using gas chromatography as part of research activities. Furthermore, it involved the application of normative documents, expert reports, and manuals for the instrumental equipment used in this analytical method. The correctness of the procedure was verified by a witness audit conducted by an expert assessor from the Czech Accreditation Institute. The analytical method for determining sulfur compounds, halogenated compounds individually and/or their sum, and formaldehyde in hydrogen was accredited by the accreditation body.

Link to research data: https://doi.org/10.5281/zenodo.17909014

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Detail

Author

  • Neuschl M.
  • Vít R.
  • Bucková M.
  • Michalicová R.
  • Jandová V.
  • Huzlík J.
  • Kučera M.
  • Souček M

Content

1. Applicability (scope of use)
2. List of abbreviations and terminology used
3. Principle
4. Technical gases and other materials
5. Apparatus
6. Equipment and aids
7. Procedure
7.1 Putting the instrument assembly into operation
7.2 Analysis procedure
7.3 Calibration procedure
7.4 Analyte measurement procedure
8. Procedure performed by
9. Information sources and standards
10. Related and follow-up SOPs
11. Document distribution and archiving
12. Appendix

Dedication

This project, Development of Methods for Hydrogen Purity Analysis Using Gas Chromatography, is co-financed with state support from the Technology Agency of the Czech Republic and the Ministry of Transport of the Czech Republic within the framework of the DOPRAVA 2030 Programme. This project was financed within the National Recovery Plan from the European Recovery and Resilience Facility.
Project: Development of Methods for Hydrogen Purity Analysis Using Gas Chromatography (CL01000029)

Colophon

ISBN 978-80-88655-53-4 (online, pdf)

Year of publication

2025